I Y. Mk Ja.rc Fl Y. . MmaYrc. Mn aJ.rc Fo .B. Jp.M. Bq rJe.a Fr C. . As gJa. r Ft K. . M.
mp (°C) nD20 (g)
Er(e)
u (f)
0
1.333
78.3
5.9
2.55
1.4475
111.0(20°) 11.2
-114.5 1.ቤተ መጻሕፍቲ ባይዱ614
24.55
5.8
10.5
14545
37.72
7.6
16.7
1.3719
6.17(20°) 5.6
-126.2 1.3856
20.45
5.5
-15.3
1.5404
13.1(20°) 5.5
-88.6
1.3993
17.51
5.8
-78.2
1.41
13.9
5.7
-117.2 1.4072
97.35 82.3 225.5 202 56.1 230 116.9 191.1 83.5 79.6 210.8 102 102.3 175.2 128.9 233 94.2 39.6 202 115.25 56.9 155.65 117.4 573 237.1 102 61.2 106.3 216 112559..285 (dec.) 84.5 77.1 180.5 168.2 188.9 66 153.6
37.78
12.4
-92.8 25.6 8.2 -24.4 -94.7 <-20 11.3 -12.75 -35.7 -86.7 5.8 -8.8 -76.9 -1.2 -4.8 7.2 -92 -94.9 19.6 -41.55 -98.05 -32.1 -84.7 -97 -14.85 -39 -63.5 -49.8 -45 -69 -64 -69 -83.55 -17 -46 -44.3 -108.4 -37.5
0.401 0.389 0.364 0.355 0.355 0.352 0.349 0.333 0.327 0.327 0.324 0.321 0.321 0.318 0.318 0.315 0.315 0.309 0.306 0.302 0.287 0.281 0.269 0.269 0.269 0.265 0.259 0.256 0.253 0.247 0.244 0.231 0.228 0.225 0.225 0.21 0.207 0.198
丙腈 叔丁醇 二甲基乙撑脲 甲基砒咯烷酮 丙酮 二甲基亚丙基脲 乙二胺 腈基苯 1,2-二氯乙烷 丁酮, 甲乙酮 硝基苯 叔戊醇 2-戊酮 四甲基脲 吗啉 六甲基磷酰胺 异戊酮 二氯甲烷 苯乙酮 吡啶 乙酸甲酯 环己酮 4-甲基-2-戊酮 1,1-二氯乙烷 喹啉 3-戊酮 氯仿 3,3-二甲基-2-丁酮 三乙二醇二甲基醚 2,4-二甲基-3-戊酮 双乙二醇二甲基醚 乙二醇二甲基醚 乙酸乙酯 邻二氯苯 2,6-二甲基-4-庚酮 双乙二醇二乙基醚 四氢呋喃 苯甲醚
126.8 84.7 31.6 131.7 155.9 169.8 188.3 74.1 101.3 87.2 55.2 106.2 55.55 258.1 344 801 90.1 110.6 138.4 140.3 46.2 76.6 88.9 214 195.8 98.4 68.7 36.1 80.7
ET (h) 1 0.799 0.79 0.762 0.722 0.713 0.704 0.667 0.664 0.657 0.654 0.651 0.648 0.617 0.608 0.602 0.568 0.565 0.552 0.546 0.506 0.5 0.491 0.488 0.481 0.463 0.46 0.444 0.42 0.41 0.407 0.404 0.401
pp.4 08-
Tabl e A-
No. Solvent Name (1) Water (2) Formamide (3) 1,2-Ethanediol (4) Methanol (5) N-Methylformamide (6) Diethylene glycol (7) TriethyIene glycol (8) 2-Methoxyethanol (9) Tetraethylene glycol (10) N-Methylacetamide (11) Ethanol (12) 2-Aminoethanol (13) Acetic acid (14) 1-Propanol (15) Benzyl alcohol (16) 1-Butanol (17) 1-Pentanol (18) 3-Methyl-1-butanol, Isoamyl alcohol (19) 2-Methyl-1-propanol, Isobutyl alcohol (20) 2-Propanolm) (21) 2-Butanol (22) Cyclohexanol (23) Propylene carbonate (24) 2-Pentanol (25) Nitromethane (26) 3-Pentanol (27) Acetonitrile (28) Dimethylsulfoxide (29) Aniline (30) SulfoIane (31) Acetic anhydride (32) N,N-Dimethyl-formamide (33) N,N-Dimethyl-acetamide
13.35
5.5
-43.8
1.3441
35.94
11.8
18.5
1.4793
46.45
13.5
-6
1.5863
6.71(30°) 5.0
28.45
1.4816(30°) 43.3(30°) 16
-73.1
1.3904
20.7(19°) 9.4
-60.4
1.4305
36.71
10.8
-20
1.4384
(34) Propanenitrile (35) 2-Methyl-2-propanol, t-Butanol (36) 1.3-Dimethyl-imidazolidin-2-one, DMEU (37) 1-Methylpyrrolidin-2-one (38) Acetone (39) 1.3-Dimethyl-2-oxo-hexahydropyrimidine, DMPU (40) 1,2-Diaminoethane (41) Cyanobenzene (42) 1,2-Dichloroethane (43) 2-Butanone (44) Nitrobenzene (45) 2-Methyl-2-butanol, t-Pentyl alcohol (46) 2-Pentanone (47) Tetramethylurea (48) Morpholine (49) Hexamethylphosphoric acid triamide, HMPT (50) 3-Methyl-2-butanone (51) Dichloromethane" (52) Acetophenone (53) Pyridine (54) Methyl acetate (55) Cyclohexanone (56) 4-Methyl-2-pentanone (57) 1,1-Dichloroethane (58) Quinoline (59) 3-Pentanone (60) Chloroform (61) 3,3-Dimethyl-2-butanone (62) Triethylene glycol dimethyl ether (63) 2,4-Dimethyl-3-pentanone (64) Diethylene glycol dimethyl ether (65) 1,2-Dimethoxyethane (66) Ethyl acetate (67) 1,2-Dichlorobenzene (68) 2,6-Dimethyl-4-heptanone (69) Diethylene glycol diethyl ether (70) Tetrahydrofuran (71) Methoxybenzene
-12.6
1.4318
37.7
7.7
-97.7
1.3284
32.66
5.7
-3.8
1.4319
182.4
12.9
-7.8
1.4475
31.69(20°) 7.7
-4.3
1.4558
23.69(20°) 10.0
-85.1
1.4021
16.93
6.8
-6.2
1.4577
19.7
10.8
30.6
1.4253(35°) 191.3(32°) 14.2
15.19
6.1
-108
1.3959
17.93
6.0
-88
1.3772
19.92
5.5
-114.7 1.3971
16.56
5.5
25.15
1.4648(25°) 15
6.2
-54.5
1.4215
64.92
16.5
1.4064
13.71
5.5
-28.55 1.3819
35.94
11.9
-75
1.4104
a Tb hCe. Rc eic Md elti Be oili Rf elat Dg ipol Rh efr Nor
碳酸二乙酯 氟苯 1,1-二氯乙烯 氯苯 溴苯 苯乙醚 碘苯 1,1,1-三氯乙烷 二噁烷 三氯乙烯 叔丁基甲醚 哌啶 二乙基胺 二苯醚 乙醚 苯 二丙醚 甲苯 对二甲苯 二丁醚 二硫化碳 四氯甲烷 三乙基胺 三丁基胺 顺十氢萘 正庚烷 正己烷 正戊烷 环己烷