combustion flask
用 IC/ISE 测定 Analyzed by IC/ISE
用用超纯水定容
Make up with ultra-purity water
转移样品溶液到容量瓶内
Transfer the sample solution into a volumetric flask
检测报告 Test Report
5.测定卤素含量 Test for Halogen Contents. 称量样品于燃烧瓶中
Weigh sample and place it in a combustion flask
充入氧气
Fill the flask with oxygen
第7页共8页 Page 7 of 8
在燃烧瓶中燃烧样品 Combust the sample in the
第3页共8页 Page 3 of 8
检测结果:
Test Results: 测试项目
含量
Tested Items
Contents
铅 Lead (Pb)
N.D.
镉 Cadmium (Cd)
N.D.
汞 Mercury (Hg)
N.D.
六价铬 Hexavalent Chromium (Cr6+)
N.D.
注：参考国际标准方法定量铅、镉、汞时，样品被完全消解。
样品信息:
Report on the submitted sample said to be:
样品名称
:聚酯
Sample Name 样品描述
:Polyester insulating varnish :棕黄色液体
Sample Description 样品型号
:Brown yellow liquid :LITON 33XX
测试仪器 Measured Equipment ICP-AES
ICP-AES
UV-Vis
GC-MSD
IC
IC
IC
ISE
检出限 Report Limit
2ppm 2ppm 2ppm 5ppm
10ppm 10ppm 10ppm 10ppm
检测报告 Test Report
报告编号:SHR08011130301002 Report No.:SHR08011130301002
氟(F)
参考 EN14582 Refer to EN14582
氯(Cl)
参考 EN14582 Refer to EN14582
溴(Br)
参考 EN14582 Refer to EN14582
碘(I)
检测结果：请参见下页.
参考 EN14582 Refer to EN14582
Test Results: Please refer to following page(s).
用去离子水定容 Make up with D.I. water
加入消解试剂 Add digestion reagent
用去离子水定容 Make up with D.I. water
第5页共8页 Page 5 of 8
在微波消解炉中消解样品 Digest sample in microwave
digestion oven
第2页共8页 Page 2 of 8
检测依据:
Test Method:
测试项目
前处理方法
Tested Items
Pretreatment Method
铅(Pb) 镉(Cd) 汞(Hg)
六价铬(Cr6+) 多溴联苯(PBBs) 多溴联苯醚(PBDEs)
参考 IEC 62321 111/54/CDV Ed.1 Sec.13 Refer to IEC 62321 111/54/CDV Ed.1 Sec.13 参考 IEC 62321 111/54/CDV Ed.1 Sec.10 Refer to IEC 62321 111/54/CDV Ed.1 Sec.10
Contents
N.D. N.D. N.D. N.D.
Note: -N.D. = Not Detected (<report limit ). -ppm = mg/kg=parts per million.
检测报告
Test Report
报告编号:SHR08011130301002 Report No.:SHR08011130301002
检测报告
Test Report
报告编号:SHR08011130301002 Report No.:SHR08011130301002
第1页共8页 Page 1 of 8
申请单位 Applicant 地址 Address
:东特涂料（太仓）有限公司 :TOTOKU TORYO (TAICANG) CO., LTD. :江苏省太仓港口开发区东方路 :Dongfang Road, Liujiagang Port Development Zone, Tiacang City, Jiangsu Province
Part No. 样品接收日期
:LITON 33XX :2008.01.10
Sample Received Date :Jan. 10, 2008
样品检测日期
:2008.01.10-2008.01.15
Testing Period 检测要求
:Jan. 10, 2008 to Jan. 15, 2008 :根据客户要求，测定所提交样品中的铅、镉、汞、六价铬、多溴联苯、 多溴联苯醚、卤素的含量。
第4页共8页 Page 4 of 8
含量 Contents
N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D. N.D.
测试项目
含量
Tested Items 卤素 Halogen 氟 Fluorin (F) 氯 Chlorin (Cl) 溴 Bromine (Br) 碘 Iodin (I) 注: -N.D. = 未检出 (小于检出限). -ppm=mg/kg=百万分之几.
加入消解剂, 加热 Add digestion
solution and heat
添加测试溶液 Add test solution
用去离子水定容 Make up with D.I. water
调整溶液 pH 至 2.0±0.5 Adjust the pH to 2.0±0.5
用去离子水定容 Make up with D.I. water
参考 IEC 62321 111/54/CDV Ed.1 Sec.9 Refer to IEC 62321 111/54/CDV Ed.1 Sec.9
参考 IEC 62321 111/54/CDV Ed.1 Sec.7 Refer to IEC 62321 111/54/CDV Ed.1 Sec.7
用 ICP-AES 测定
Analyzed by ICP-AES
2.测定 Hg 含量。 Test for Hg Content.
称量样品于微波消解容器中 Weigh sample and place in a microwave digestion vessel
用 ICP-AES 测定 Analyzed by ICP-AES
主 检: Tested by
审 核: Inspected by
签 发: Approved by
技术经理 Technical Manager
签发日期: Date
2008.01.15 Jan. 15, 2008
检测报告
Test Report
报告编号:SHR08011130301002 Report No.:SHR08011130301002
浓缩萃取液 Concentrate the extract
转移萃取溶液至容量瓶内 Transfer the extract into a
volumetric flask
检测报告
Test Report
报告编号:SHR08011130301002 Report No.:SHR08011130301002
4.测定多溴联苯和多溴联苯醚含量 Test for PBBs /PBDEs Contents. 称量样品于套管中
Weigh sample and place it in a thimble
用有机溶剂萃取 Extracted with organic solvent
用 GC-MSD 分析 Analyzed by GC-MSD
用有机溶剂定容 Make up with organic solvent
第6页共8页 Page 6 of 8
调整溶液 pH 值至 7.5±0.5 Adjust the pH to 7.5±0.5
转移溶液到容量瓶 Transfer the extract into a
volumetric flask
用 UV-Vis 测定 Analyzed by UV-Vis
报告编号:SHR08011130301002 Report No.:SHR08011130301002
样品照片 Photo of the sample
含量 Contents
N.D. N.D. N.D. N.D. N.D. N.D.告
Test Report
报告编号:SHR08011130301002 Report No.:SHR08011130301002
测试项目 Tested Items 多溴联苯醚 polybrominated Diphenyl Ethers(PBDEs) 一溴联苯醚 Monobromodiphenyl ether 二溴联苯醚 Dibromobiphenyl ether 三溴联苯醚 Tribromobiphenyl ether 四溴联苯醚 Tetrabromobiphenyl ether 五溴联苯醚 Pentabromobiphenyl ether 六溴联苯醚 Hexabromobiphenyl ether 七溴联苯醚 Heptabromobiphenyl ether 八溴联苯醚 Octabromobiphenyl ether 九溴联苯醚 Nonabromobiphenyl ether 十溴联苯醚 Decabromobiphenyl ether